HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20223186, compound → HCID 68828128, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20223186 | HCID 20223186 | — |
| Solvent | Isobutanol | HCID 6560 | — |
| Product | HCID 68828128 | HCID 68828128 | — |
Reaction Steps
33.2 g (0.2 mol) bicyclo[2.2.1]heptane dicarboxylic anhydride was charged to 300 ml isobutyl alcohol in a 1 L round bottom flask. The system was refluxed for 2 hours with magnetic stirring. The solvent was then removed by rotary evaporator. The system was then dried and grounded. The product was characterized using FTIR and GC-MS. The yield was quantitative.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07566797B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-5a2145c2f6574ee49dadf28c5d2306b7 |
| Source note | uspto-grants-2009_07 |