Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2307528Generated: October 31, 2026

Benzoyl chloride, 3,4-dichloro- → HCID 86756240, compound

https://huagongshe.com/reaction/2307528

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzoyl chloride, 3,4-dichloro-HCID 76403—
ReactantHCID 69435312HCID 69435312—
SolventPyridineHCID 1049—
SolventDichloromethaneHCID 6344—
ProductHCID 86756240HCID 8675624029.7%

Reaction Steps

A mixture of cis and trans 2-benzoyloxymethyl-5-hydroxy-1,3-oxathiolane (as prepared in example 1) (8.99 g, 39.8 mmol) was reacted with 8.3 g (39.6 mmol) of 3,4-dichlorobenzoylchloride in dichloromethane (30 mL) and pyridine (9.6 mL) as described in Example 2 to yield 4.86 g of the desired compounds in 1:1 ratio.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06831174B2
Source datasetuspto-grants-2004_12
ORD IDord-6160484691094db38cfa7c4a1e8319c0
Source noteuspto-grants-2004_12