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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2307556Generated: November 1, 2026

Potassium Carbonate → Methyl 3'-[3,4-bis(1-phenylmethanoyloxymethyl)benzyloxy]-2,2'-dimethylbiphenyl-4-carboxylate

https://huagongshe.com/reaction/2307556

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactant3,4-Bis(benzoyloxymethyl)benzyl bromideHCID 22345618—
ReactantMethyl 3'-hydroxy-2,2'-dimethylbiphenyl-4-carboxylateHCID 22606889—
ProductMethyl 3'-[3,4-bis(1-phenylmethanoyloxymethyl)benzyloxy]-2,2'-dimethylbiphenyl-4-carboxylateHCID 22606870—

Reaction Steps

In a manner similar to that of Example 1(i), by reaction of 515 mg (2 mmol) of methyl 3′-hydroxy-2,2′-dimethylbiphenyl-4-carboxylate with 880 mg (2 mmol) of 3,4-bis(benzoyloxymethyl)benzyl bromide and 300 mg (2.2 mmol) of potassium carbonate, the desired product is obtained in the form of a colourless oil (m=1.22 g; Y=99%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06831106B1
Source datasetuspto-grants-2004_12
ORD IDord-671fe4123c53468cb1bac241042bcb7b
Source noteuspto-grants-2004_12