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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2307565Generated: October 31, 2026

Potassium Carbonate → Methyl 5'-[3,4-bis(1-phenylmethanoyloxymethyl)-benzyloxy]-2,2'-dimethylbiphenyl-4-carboxylate

https://huagongshe.com/reaction/2307565

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactant3,4-Bis(benzoyloxymethyl)benzyl bromideHCID 22345618—
ReactantMethyl 5'-hydroxy-2,2'-dimethylbiphenyl-4-carboxylateHCID 22606936—
ProductMethyl 5'-[3,4-bis(1-phenylmethanoyloxymethyl)-benzyloxy]-2,2'-dimethylbiphenyl-4-carboxylateHCID 22606884—

Reaction Steps

In a manner similar to that of Example 1(i), by reaction of 2.24 g (8.7 mmol) of methyl 5′-hydroxy-2,2′-dimethylbiphenyl-4-carboxylate with 4.20 mg (9.6 mmol) of 3,4-bis(benzoyloxymethyl)benzyl bromide and 1.26 g (9 mmol) of potassium carbonate, the desired product is obtained in the form of a colourless oil (m=5.34 g; Y=99%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06831106B1
Source datasetuspto-grants-2004_12
ORD IDord-1a401cad74374004bf05d3b515ce2317
Source noteuspto-grants-2004_12