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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2307570Generated: October 26, 2026

Potassium Carbonate → Methyl 3'-(3,4-bis(1-phenylmethanoyloxymethyl)-benzyloxy]-2,6-dimethylbiphenyl-4-carboxylate

https://huagongshe.com/reaction/2307570

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactant3,4-Bis(benzoyloxymethyl)benzyl bromideHCID 22345618—
ReactantMethyl 3'-hydroxy-2,6-dimethylbiphenyl-4-carboxylateHCID 22606868—
ProductMethyl 3'-(3,4-bis(1-phenylmethanoyloxymethyl)-benzyloxy]-2,6-dimethylbiphenyl-4-carboxylateHCID 22606946—

Reaction Steps

In a manner similar to that of Example 1(i), by reaction of 4.49 g (17.5 mmol) of methyl 3′-hydroxy-2,6-dimethylbiphenyl-4-carboxylate with 8.46 g (19 mmol) of 3,4-bis(benzoyloxymethyl)benzyl bromide and 2.54 g (18 mmol) of potassium carbonate, the desired product is obtained in the form of a yellow oil (m=7.4 g; Y=69%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06831106B1
Source datasetuspto-grants-2004_12
ORD IDord-54586624f33b45df9c957176a61d95b0
Source noteuspto-grants-2004_12