HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 22606926, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3-Formylphenylboronic acid | HCID 2734356 | — |
| Reactant | HCID 22345619 | HCID 22345619 | — |
| Catalyst | HCID 178418397 | HCID 178418397 | — |
| Product | HCID 22606926 | HCID 22606926 | — |
Reaction Steps
In a manner similar to that of Example 1(h), by reaction of 6.6 g (44 mmol) of 3-formylbenzeneboronic acid and 10 g (37 mmol) of 2-(4-bromo-3-methylphenyl)-2-ethyl-[1,3]dioxolane with 45 mL of 2.0M potassium carbonate and 2.14 g of tetrakis(triphenylphosphine)palladium, the desired product is obtained in the form of a thick oil (m=9.1 g; Y=84%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06831106B1 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-75d676d9279d407684250c5bf5f84c0f |
| Source note | uspto-grants-2004_12 |