Dimethyl Disulfide → 3-(Methylsulfanyl)benzaldehyde

HRID 2307688Notes

Reaction equation

HRID 2307688 reaction equation

Br[C:2]1[CH:3]=[C:4]([CH:8]2[O:12]CCO2)[CH:5]=[CH:6][CH:7]=1.[CH3:13][S:14]SC>>[CH3:13][S:14][C:2]1[CH:3]=[C:4]([CH:5]=[CH:6][CH:7]=1)[CH:8]=[O:12]

Participants

3

Reactant 2

HCID 12232Dimethyl Disulfide

HCID 873062-(3-Bromophenyl)-1,3-dioxolane

Product 1

HCID 127211713-(Methylsulfanyl)benzaldehyde

Procedure

2-(3-Bromophenyl)-1,3-dioxolane and dimethyl disulfide were processed as described in Example 71A to provide the title compound.

Sources & evidence

ORD record: ord-bc85289ae91442cbb7d5cc9335a78b56
Source dataset: uspto-grants-2004_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06831193B2

Reaction notes

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