3,4-Dichlorobenzeneboronic acid → HCID 10232743, compound

HRID 2307705Notes

Reaction equation

HRID 2307705 reaction equation
Br[C:2]1[CH:3]=[C:4]([CH:34]=[CH:35][CH:36]=1)[CH2:5][N:6]([C@@H:24]1[C:33]2[C:28](=[CH:29][CH:30]=[CH:31][CH:32]=2)[CH2:27][CH2:26][CH2:25]1)[C:7]([C:9]1[CH:14]=[C:13]([C:15]([OH:17])=[O:16])[C:12]([C:18]([OH:20])=[O:19])=[CH:11][C:10]=1[C:21]([OH:23])=[O:22])=[O:8].[Cl:37][C:38]1[CH:39]=[C:40](B(O)O)[CH:41]=[CH:42][C:43]=1[Cl:44]>>[Cl:37][C:38]1[CH:39]=[C:40]([C:2]2[CH:36]=[CH:35][CH:34]=[C:4]([CH2:5][N:6]([C@@H:24]3[C:33]4[C:28](=[CH:29][CH:30]=[CH:31][CH:32]=4)[CH2:27][CH2:26][CH2:25]3)[C:7]([C:9]3[CH:14]=[C:13]([C:15]([OH:17])=[O:16])[C:12]([C:18]([OH:20])=[O:19])=[CH:11][C:10]=3[C:21]([OH:23])=[O:22])=[O:8])[CH:3]=2)[CH:41]=[CH:42][C:43]=1[Cl:44]

Participants

3

Reactant 2

HCID 27343303,4-Dichlorobenzeneboronic acidHCID 10144017HCID 10144017, compound

Product 1

HCID 10232743HCID 10232743, compound

Procedure

The product from Example 15B (165 mg, 0.3 mmol) and 3,4-dichlorophenylboronic acid were processed as described in Example 85 to provide the title compound.

Sources & evidence

ORD record
ord-5813ba8374e845f9a24464d465228f10
Source dataset
uspto-grants-2004_12
Patent number
US06831193B2

Reaction notes

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