HCID 10144017, compound → HCID 10311933, compound

HRID 2307708Notes

Reaction equation

HRID 2307708 reaction equation
Br[C:2]1[CH:3]=[C:4]([CH:34]=[CH:35][CH:36]=1)[CH2:5][N:6]([C@@H:24]1[C:33]2[C:28](=[CH:29][CH:30]=[CH:31][CH:32]=2)[CH2:27][CH2:26][CH2:25]1)[C:7]([C:9]1[CH:14]=[C:13]([C:15]([OH:17])=[O:16])[C:12]([C:18]([OH:20])=[O:19])=[CH:11][C:10]=1[C:21]([OH:23])=[O:22])=[O:8].[S:37]1[CH:41]=[CH:40][C:39](C2C=C(B(O)O)C=CC=2)=[CH:38]1>>[C@@H:24]1([N:6]([CH2:5][C:4]2[CH:34]=[CH:35][CH:36]=[C:2]([C:39]3[CH:40]=[CH:41][S:37][CH:38]=3)[CH:3]=2)[C:7]([C:9]2[CH:14]=[C:13]([C:15]([OH:17])=[O:16])[C:12]([C:18]([OH:20])=[O:19])=[CH:11][C:10]=2[C:21]([OH:23])=[O:22])=[O:8])[C:33]2[C:28](=[CH:29][CH:30]=[CH:31][CH:32]=2)[CH2:27][CH2:26][CH2:25]1

Participants

3

Reactant 2

HCID 10144017HCID 10144017, compoundHCID 22608023HCID 22608023, compound

Product 1

HCID 10311933HCID 10311933, compound

Procedure

The product from Example 15B (165 mg, 0.3 mmol) and 3-(3-thienyl)phenylboronic acid were processed as described in Example 85 to provide the title compound.

Sources & evidence

ORD record
ord-63581a2f73714d68a5768a5589e88de2
Source dataset
uspto-grants-2004_12
Patent number
US06831193B2

Reaction notes

Loading…