HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Bromophenyl)methanethiol → (Z)-2,3-dimethylstyryl-4-bromobenzylsulfide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Bromophenyl)methanethiol | HCID 271218 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 1-Ethynyl-2,3-dimethylbenzene | HCID 22603764 | — |
| Product | (Z)-2,3-dimethylstyryl-4-bromobenzylsulfide | HCID 86593388 | — |
Reaction Steps
A solution of 2,3-dimethylphenylacetylene (0.02 mol), 4-bromobenzyl mercaptan (0.02 mol) and metallic sodium (0.02 g atom) is subjected to the General Procedure to form (Z)-2,3-dimethylstyryl-4-bromobenzylsulfide. The title compound is obtained following oxidation of the sulfide, according to the General Procedure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06833480B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-6dca270ea1694e7ab1a54f00a0590ada |
| Source note | uspto-grants-2004_12 |