HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichlorobenzenemethanethiol → (Z)-2,4-difluorostyryl-2,4-dichlorobenzylsulfide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichlorobenzenemethanethiol | HCID 95756 | — |
| Reactant | 1-Ethynyl-2,4-difluorobenzene | HCID 5063820 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Product | (Z)-2,4-difluorostyryl-2,4-dichlorobenzylsulfide | HCID 86593390 | — |
Reaction Steps
A solution of 2,4-difluorophenylacetylene (0.02 mol), 2,4-dichlorobenzyl mercaptan (0.02 mol) and metallic sodium (0.02 g atom) is subjected to the General Procedure to form (Z)-2,4-difluorostyryl-2,4-dichlorobenzylsulfide. The title compound is obtained following oxidation of the sulfide, according to the General Procedure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06833480B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-2991cf0ceaec48ceaa11d44ba09043cc |
| Source note | uspto-grants-2004_12 |