HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium → (Z)-3-methoxy-4-acetoxystyryl-2-chloro-4-methoxybenzylsulfide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 22603791 | HCID 22603791 | — |
| Reactant | 3-Methoxy-4-acetoxyphenylacetylene | HCID 22603806 | — |
| Product | (Z)-3-methoxy-4-acetoxystyryl-2-chloro-4-methoxybenzylsulfide | HCID 86593397 | — |
Reaction Steps
A solution of 3-methoxy-4-acetoxyphenylacetylene (0.02 mol), 2-chloro-4-methoxybenzyl mercaptan (0.02 mol) and metallic sodium (0.02 g atom) is subjected to the General Procedure to form (Z)-3-methoxy-4-acetoxystyryl-2-chloro-4-methoxybenzylsulfide. The title compound is obtained following oxidation of the sulfide, according to the General Procedure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06833480B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-65d2f551aa5241bd8d514f1a5a39b5b3 |
| Source note | uspto-grants-2004_12 |