(4-Methoxyphenyl)boronic acid → HCID 10086722, compound

Participants

Reaction Steps

Starting from 2-(3-bromo-5-iodo-4-methylthien-2-yl)-1,3-dioxolane (9.3 g, 25 mmol) and substituting 3-methoxyphenylboronic acid (4.1 g, 27 mmol) in place of 4-methoxyphenylboronic acid (Example 1, Step 1) and substituting 4-methoxyphenylboronic acid in place of 3-methoxyphenylboronic acid (Example 1, Step 2), the title compound (0.40 g, 85%, m.p. 208-10° C.) was synthesized in essentially the same manner as described in Example 1.

Provenance & Evidence