HuagongsheHuagongshe Chemistry Print Report · For research reference only
(5-Methoxy-2-methylphenyl)boronic acid → HCID 10381607, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (5-Methoxy-2-methylphenyl)boronic acid | HCID 17750868 | — |
| Reactant | HCID 22601714 | HCID 22601714 | — |
| Product | HCID 10381607 | HCID 10381607 | 89% |
Reaction Steps
Starting from 2-[3-bromo-5-(4-methoxyphenyl)-4-methylthien-2-yl]-1,3-dioxolane (1.1 g, 3.0 mmol, made in Example 1, Step 1) and substituting 5-methoxy-2-methylphenylboronic acid (0.55 g, 3.3 mmol) in place of 3-methoxyphenylboronic acid (Step 2), the title compound (0.49 g, 89%, m.p. 204-07° C.) was synthesized in essentially the same manner as described in Example 1, Steps 2-4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06835745B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-458276d48d0042ccbafacb2e3a6fdf66 |
| Source note | uspto-grants-2004_12 |