(4-Methoxy-2-methylphenyl)boronic acid → HCID 9997478, compound

Participants

Reaction Steps

Starting from 2-[3-bromo-5-(3-fluoro-4-methoxyphenyl)-4-methylthien-2-yl]-1,3-dioxolane (0.90 g, 2.4 mmol, made in Example 8, Step 1) and substituting 4-methoxy-2-methylphenylboronic acid (0.44 g, 2.7 mmol) in place of 4-methoxyphenylboronic acid (Step 2), the title compound (0.31 g, 76%, m.p. 227-30° C.) was synthesized in essentially the same manner as described in Example 1, Steps 2-4.

Provenance & Evidence