HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluoro-4-methoxyphenylboronic acid → HCID 10405103, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluoro-4-methoxyphenylboronic acid | HCID 2782194 | — |
| Reactant | HCID 22601711 | HCID 22601711 | — |
| Product | HCID 10405103 | HCID 10405103 | 67% |
Reaction Steps
Starting from 2-[3-bromo-5-(4-methoxy-2-methylphenyl)-4-methylthien-2-yl]-1,3-dioxolane (0.96 g, 2.6 mmol, made in Example 11, Step 1) and substituting 3-fluoro-4-methoxyphenylboronic acid (0.57 g, 3.4 mmol) in place of 3-methoxyphenylboronic acid (Step 2), the title compound (0.40 g, 67%) was synthesized in essentially the same manner as described in Example 1, Steps 2-4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06835745B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-3d3cc9ab262e4631b6dffdd56619a887 |
| Source note | uspto-grants-2004_12 |