HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Methoxyphenyl)boronic acid → HCID 10360168, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Methoxyphenyl)boronic acid | HCID 201262 | — |
| Reactant | 3-Chloro-4-methoxybenzeneboronic acid | HCID 3247522 | — |
| Reactant | HCID 22601716 | HCID 22601716 | — |
| Product | HCID 10360168 | HCID 10360168 | 75% |
Reaction Steps
Starting from 2-(3-bromo-5-iodo-4-methylthien-2-yl)-1,3-dioxolane (2.5 g, 6.7 mmol) and 3-chloro-4-methoxyphenylboronic acid (1.5 g, 8.0 mmol) in place of 4-methoxyphenylboronic acid (Step 1), and substituting 4-methoxyphenylboronic acid in place of 3-methoxyphenylboronic acid (Step 2), the title compound (0.41 g, 75%) was synthesized in essentially the same manner as described in Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06835745B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-c73d65f3b5f5424ea50db24b5cbfb487 |
| Source note | uspto-grants-2004_12 |