HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22601390, compound → HCID 22601475, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22601390 | HCID 22601390 | — |
| Catalyst | Manganese dioxide | HCID 14801 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22601475 | HCID 22601475 | 82.5% |
Reaction Steps
Reaction of 3-Hydroxymethyl-N-phenyl-benzenesulfonamide (crude from previous step, 1.36 mmol), MnO2 (1.40 g, 13.60 mmol) in CH2Cl2 (10 mL) at 40° C. under N2 overnight gave the title compound (293 mg, 82%) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06835731B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-8c86eed5e80144d3aab00561883a19c8 |
| Source note | uspto-grants-2004_12 |