HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22601494, compound → N-benzyl-3-formyl-benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22601494 | HCID 22601494 | — |
| Catalyst | Manganese dioxide | HCID 14801 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | N-benzyl-3-formyl-benzenesulfonamide | HCID 10636117 | 85% |
Reaction Steps
Reaction N-Benzyl-3-hydroxymethyl-benzenesulfonamide (crude from previous step, 1.36 mmol), MnO2 (1.40 g, 13.60 mmol) in CH2Cl2 (10 mL) at 40° C. under N2 overnight gave the title compound (317 mg, 85%) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06835731B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-02be9eaa93d642b18edc028ecdd97956 |
| Source note | uspto-grants-2004_12 |