N-tert-butylhydroxylamine → HCID 85060213, compound

HRID 2308369Notes

Reaction equation

HRID 2308369 reaction equation
[C:1]([C:5]1[CH:6]=[C:7]([CH:10]=[C:11]([C:20]([CH3:23])([CH3:22])[CH3:21])[C:12]=1[O:13][CH2:14][O:15][CH2:16][CH2:17][O:18][CH3:19])[CH:8]=O)([CH3:4])([CH3:3])[CH3:2].[C:24]([NH:28][OH:29])([CH3:27])([CH3:26])[CH3:25]>C1C=CC=CC=1>[CH3:19][O:18][CH2:17][CH2:16][O:15][CH2:14][O:13][C:12]1[C:11]([C:20]([CH3:22])([CH3:21])[CH3:23])=[CH:10][C:7]([CH:8]=[N+:28]([C:24]([CH3:27])([CH3:26])[CH3:25])[O-:29])=[CH:6][C:5]=1[C:1]([CH3:3])([CH3:2])[CH3:4]

Participants

4

Reactant 2

HCID 98586N-tert-butylhydroxylamineHCID 15027766HCID 15027766, compound

Product 1

HCID 85060213HCID 85060213, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

The title compound was prepared in benzene with 3,5-di-tert-butyl-4-(2-methoxy)ethoxymethoxybenzaldehyde and tert-butylhydroxylamine using the procedure described in Example 16. The title compound was isolated (70.1% yield) as a white solid, m.p. 169.6-173.5° C.

Sources & evidence

ORD record
ord-1583bc97a13a4e229680b2483da1e4d3
Source dataset
uspto-grants-2004_12
Patent number
US06835754B2

Reaction notes

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