4-Fluorobenzoyl chloride → HCID 178489161, compound

HRID 2308448Notes

Reaction equation

HRID 2308448 reaction equation
[CH3:1][O:2][C:3]1[C:8]2[N:9]=[C:10]([NH2:12])[S:11][C:7]=2[C:6]([C:13]2[NH:17][N:16]=[N:15][N:14]=2)=[CH:5][CH:4]=1.[F:18][C:19]1[CH:27]=[CH:26][C:22]([C:23](Cl)=[O:24])=[CH:21][CH:20]=1>N1C=CC=CC=1>[F:18][C:19]1[CH:27]=[CH:26][C:22]([C:23]([NH:12][C:10]2[S:11][C:7]3[C:6]([C:13]4[NH:14][N:15]=[N:16][N:17]=4)=[CH:5][CH:4]=[C:3]([O:2][CH3:1])[C:8]=3[N:9]=2)=[O:24])=[CH:21][CH:20]=1

Participants

4

Reactant 2

HCID 678794-Fluorobenzoyl chlorideHCID 178489162HCID 178489162, compound

Product 1

HCID 178489161HCID 178489161, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

Using 4-methoxy-7-(1H-tetrazol-5-yl)-benzothiazol-2-ylamine and 4-fluoro-benzoyl chloride in pyridine the title compound was obtained as a tan solid (70% yield), MS: m/e=371.2 (M+H+).

Sources & evidence

ORD record
ord-d39d8985af024840804f70612cfe0b4d
Source dataset
uspto-grants-2004_12
Patent number
US06835732B2

Reaction notes

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