HuagongsheHuagongshe Chemistry Print Report · For research reference only
Picolyl chloride hydrochloride → 2-Dimethylaminopyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Picolyl chloride hydrochloride | HCID 23392 | — |
| Reactant | Methylamine ethanol | HCID 22028356 | — |
| Product | 2-Dimethylaminopyridine | HCID 21885 | 20% |
Reaction Steps
Using 2-chloromethyl-pyridine hydrochloride salt and 33% methylamine/EtOH the title compound was obtained as a colourless liquid (0.1 mm Hg, 47-48° C.) (20% yield), MS: m/e=93.1 (M—NHCH3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06835732B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-96af87c7418a4e7ab25d059986a7f661 |
| Source note | uspto-grants-2004_12 |