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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2308887Generated: November 2, 2026

Acetic Anhydride → HCID 14802198, compound

https://huagongshe.com/reaction/2308887

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetic AnhydrideHCID 7918—
Reactant4,6,7-Trimethyl-2-propyl-2H-1,3-benzoxathiol-5-olHCID 127576—
SolventPyridineHCID 1049—
ProductHCID 14802198HCID 1480219895.6%

Reaction Steps

A mixture of 1.6 g of 5-hydroxy-4,6,7-trimethyl-2-propyl-1,3-benzoxathiole (prepared as described in Example 42), 0.8 g of acetic anhydride and 10 ml of pyridine was reacted at room temperature for 15 hours and the reaction mixture was then treated with purified in the same manner as described in Example 4, to give 1.8 g of the title compound as a pale yellow oily substance.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04691027
Source datasetuspto-grants-1987_09
ORD IDord-2840281413174e79899bb5d150a47e91
Source noteuspto-grants-1987_09