HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Propanediol → 2-(3-Chlorophenyl)-1,3-dioxane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Propanediol | HCID 10442 | — |
| Reactant | 3-Chlorobenzaldehyde | HCID 11477 | — |
| Product | 2-(3-Chlorophenyl)-1,3-dioxane | HCID 11788854 | — |
Reaction Steps
The title compound was prepared as a colourless oil, bp 95°-102° C./0.2 mm, from 3-chlorobenzaldehyde (24 g) and 1,3-propanediol (20 g) by an analogous procedure to that described in Example X 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04692465 |
| Source dataset | uspto-grants-1987_09 |
| ORD ID | ord-d384641d7bba49699194fda7bad0a20a |
| Source note | uspto-grants-1987_09 |