HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Trifluoromethyl)acrylic acid → 3-Acetylthio-2-trifluoromethylpropanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Trifluoromethyl)acrylic acid | HCID 587694 | — |
| Reactant | HCID 178473673 | HCID 178473673 | — |
| Product | 3-Acetylthio-2-trifluoromethylpropanoic acid | HCID 12833014 | — |
Reaction Steps
A mixture of thiolactic acid (50 g.) and 2-(trifluoromethyl)acrylic acid [M. W. Buxton, et al., J. Chem. Soc., 366 (1954)] (66 g.) is heated on the steam bath for one hour and then stored at room temperature for eighteen hours. The reaction mixture is distilled in vacuo to give 3-acetylthio-2-trifluoromethylpropanoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04692458 |
| Source dataset | uspto-grants-1987_09 |
| ORD ID | ord-31a23a5294854dea8affc28626ca90ba |
| Source note | uspto-grants-1987_09 |