HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 14047789, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 2,6-Di-tert-butyl-4-mercaptophenol | HCID 70370 | — |
| Reactant | Chloromethylphthalimide | HCID 87154 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 14047789 | HCID 14047789 | — |
Reaction Steps
A vessel was charged with 12.19 grams of 3,5-di-tert-butyl-4-hydroxybenzene thiol and 3.30 grams of potassium hydroxide dissolved in 50 ml of acetone and 2 ml of water at 0° C. which was mixed with 10.0 grams of N-(chloromethyl)phthalimide. After stirring for one hour, the precipitated product was removed by filtration and then recrystallized from ethyl acetate-hexane to give 14.9 grams of produt, m.p. 151°-53° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04692532 |
| Source dataset | uspto-grants-1987_09 |
| ORD ID | ord-c82174b5f02b4ad78684a901829fa7a5 |
| Source note | uspto-grants-1987_09 |