huagongshe.com
HRID2309120

反应详情

EQUATION

反应方程式

HRID 2309120 的结构方程式

REACTANTS

反应物

3
结构：[K+].[OH-]
HCID14797

Potassium hydroxide

HKO

结构：O=C1c2ccccc2C(=O)N1CCl
HCID87154

2-(Chloromethyl)-1H-isoindole-1,3(2H)-dione

C9H6ClNO2

结构：Cc1cc(S)cc(C(C)(C)C)c1O
HCID13547656

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(SCN2C(=O)c3ccccc3C2=O)cc(C(C)(C)C)c1O
HCID14047795

未命名化合物

收率 46.3%

PROCEDURE

实验过程

The procedure of Example 1 was repeated using 8.46 grams of 3-methyl-4-hydroxy-5-tert-butylbenzenethiol, 1.72 grams of potassium hydroxide, and 8.43 grams of N-(chloromethyl) phthalimide . Recrystallization from ethyl acetate-heptane afforded 7.1 grams of product with m.p. 114°-116° C.

WORKUP

后处理

  1. customRecrystallization from ethyl acetate-heptane