Benzoate → HCID 18609748, compound

Participants

Reaction Steps

A solution of 0.55 g. of the alcohol prepared according to Reference Example 1(m) in 4 ml. of pyridine is combined with 0.5 ml. of benzoyl chloride. The mixture is agitated for 4 hours at 25°, combined with 0.4 ml. of water, agitated for 2 hours, diluted with ether, and the mixture is shaken in succession with water, 5% sulfuric acid, water, 4% sodium bicarbonate solution, and three times with water. After drying over magnesium sulfate the mixture is evaporated under vacuum, thus obtaining 720 mg. of the benzoate as a colorless oil.

Provenance & Evidence