HuagongsheHuagongshe Chemistry Print Report · For research reference only
(S)-2-(2-((tert-Butoxycarbonyl)amino)propanamido)acetic acid → Boc-Ala-Gly-Val-Pro-Gly-Phe-Gly-Val-Gly-OH
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (S)-2-(2-((tert-Butoxycarbonyl)amino)propanamido)acetic acid | HCID 192414 | — |
| Reactant | Boc-Ala-Gly-Val-Pro-Gly-Phe-Gly-Val-Gly-OBzl | HCID 131715251 | — |
| Product | Boc-Ala-Gly-Val-Pro-Gly-Phe-Gly-Val-Gly-OH | HCID 131715250 | — |
Reaction Steps
The nonapeptide benzylester (IX) was hydrogenated as described under VIII to obtain the acid in quantitative yield. Rf3 0.24. Anal. calcd. for C40H61N9O12 ·H2O: C 55.09, H 7.16, N 14.3%. Found: C 54.69, H 7.16, N 13.81%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04693718 |
| Source dataset | uspto-grants-1987_09 |
| ORD ID | ord-2553320f547c4f47840806d0c70941be |
| Source note | uspto-grants-1987_09 |