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HRID2309219

反应详情

EQUATION

反应方程式

HRID 2309219 的结构方程式

REACTANTS

反应物

3
结构：O
HCID962

Water

H2O

结构：CC(=O)[O-].CC(=O)[O-].O.O.[Zn+2]
HCID2724192

Zinc(II) acetate dihydrate

C4H10O6Zn

结构：CC[C@@H](C(=O)[C@@H](C)[C@@H](O)[C@@H](C)[C@H]1O[C@@H](CC(=O)OO)[C@H](C)C[C@@H]1C)[C@H]1O[C@](C)([C@]2(O)O[C@](CC)([C@@H](O)CC)C[C@H]2C)C[C@@H]1C.[Na]
HCID86741790

未命名化合物

PRODUCTS

生成物

1
结构：CC[C@@H](C(=O)[C@@H](C)[C@@H](O)[C@@H](C)[C@H]1O[C@@H](CC(=O)OO)[C@H](C)C[C@@H]1C)[C@H]1O[C@](C)([C@]2(O)O[C@](CC)([C@@H](O)CC)C[C@H]2C)C[C@@H]1C.[Zn]
HCID86741791

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

A mixture of 13.0 g of sodium lysocellin and 5.0 g zinc acetate dihydrate in 150 ml of acetone was stirred at ambient temperature for approximately 18 hours. Stirring was continued and two volumes of water were added slowly to precipitate the zinc salt. The product was isolated and dried (14.0 g). The zinc salt was recrystallized from acetone. The resulting solid product had a melting point of 102.0° C. Analysis: % Zn calculated (4.95); Found (4.37).

WORKUP

后处理

  1. stirringStirring
  2. customto precipitate the zinc salt
  3. customThe product was isolated
  4. customdried (14.0 g)
  5. customThe zinc salt was recrystallized from acetone