化工社化工社 化学情報印刷レポート · 研究参考用
Bacitracin → Bacitracin Sodium Lysocellin
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Bacitracin | HCID 10909430 | — |
| 反応物 | Sodium lysocellin | HCID 86741790 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | Bacitracin Sodium Lysocellin | HCID 86741797 | 89.4% |
反応手順
A solution of 13.0 g sodium lysocellin in 300 ml of methanol was stirred while 28.0 g bacitracin (reg) was added. Stirring was continued until solution of solids was complete. The resulting solution was held at room temperature for 18 hours. A precipitate formed and was collected on a filter, rinsed with methanol and dried to give 36.5 g of an amorphous product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04693992 |
| 出典データセット | uspto-grants-1987_09 |
| ORD ID | ord-768c058b0a164c88912dc195a1014ae8 |
| 出典メモ | uspto-grants-1987_09 |