HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2309254Generated: November 3, 2026
Triethylamine → 4-(6-Methacryloxyhexyloxy)-4'-nitrobiphenyl
https://huagongshe.com/reaction/2309254
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methacryloyl chloride | HCID 13528 | — |
| Reactant | 4-(6-Hydroxyhexyloxy)-4'-nitrobiphenyl | HCID 19779569 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 4-(6-Methacryloxyhexyloxy)-4'-nitrobiphenyl | HCID 19779570 | — |
Reaction Steps
4-(6-Hydroxyhexyloxy)-4'-nitrobiphenyl (22 g) is dissolved in 500 ml of dry dioxane and heated to 45° C. A 14 g quantity of triethylamine is added, then a solution of 10.5 g of methacryloyl chloride in an equal volume of dioxane is added dropwise while maintaining the reaction medium temperature at 45° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04694066 |
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| Source dataset | uspto-grants-1987_09 |
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| ORD ID | ord-5d971bf76f85425ca2bfc1114254aaa6 |
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| Source note | uspto-grants-1987_09 |
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