HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → Benzenesulfonamide, 2-(4-isoxazolyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | 2-(4-Isoxazolyl)benzenesulfonyl chloride | HCID 13489812 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | Benzenesulfonamide, 2-(4-isoxazolyl)- | HCID 13489819 | — |
Reaction Steps
By the procedure of Example 5, 15 g of 2-(isoxazol-4-yl)benzenesulfonyl chloride prepared in Example 12 was reacted with 30 ml of concentrated ammonium hydroxide in 150 ml of tetrahydrofuran to give, after recrystallization from 2-propanol, 11 g of the title compound; m.p. 165°-167° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04695311 |
| Source dataset | uspto-grants-1987_09 |
| ORD ID | ord-2dac79afb3234d2d8926f9800c6186e5 |
| Source note | uspto-grants-1987_09 |