HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylhydrazine → HCID 3544471, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylhydrazine | HCID 6061 | — |
| Reactant | HCID 3557290 | HCID 3557290 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 3544471 | HCID 3544471 | 92.1% |
Reaction Steps
A solution of 60 g of 3-(dimethylamino)-2-(2-nitrophenyl)acrolein (see Example 10) and 16.1 g of methylhydrazine in 200 ml of toluene was refluxed for 10 hours, then concentrated to dryness in vacuo. The residue was recrystallized from 1-chlorobutane/hexane (about 1:1) to yield 51 g of the title compound; m.p. 41°-44° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04695311 |
| Source dataset | uspto-grants-1987_09 |
| ORD ID | ord-22b173c1c5154cdb8d514eaeeb550f54 |
| Source note | uspto-grants-1987_09 |