HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Carbonate → HCID 13603315, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Carbonate | HCID 7766 | — |
| Reactant | HCID 13603314 | HCID 13603314 | — |
| Product | HCID 13603315 | HCID 13603315 | 85% |
Reaction Steps
Starting with 1.5 g. (6.98 mmoles) of 2-methyl-5-ethyl-6-oxo-6,7-dihydro-furo[2,3-f]indole and 2.47 g. (20.9 mmoles) of diethyl carbonate, and following the procedure of Preparation C, 1.7 g. (85% yield) of the desired intermediate was obtained, m.p. 82°-90° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04695571 |
| Source dataset | uspto-grants-1987_09 |
| ORD ID | ord-47a1d9eb6a184f32814d241397dbf748 |
| Source note | uspto-grants-1987_09 |