Methyl iodide → HCID 20185208, compound

HRID 2309417Notes

Reaction equation

HRID 2309417 reaction equation
[CH3:1][N:2]([CH2:4][CH:5]1[C:17](=[O:18])[C:16]2[C:15]3[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=3)[NH:9][C:8]=2[CH2:7][CH2:6]1)[CH3:3].[I:19][CH3:20]>>[I-:19].[CH3:3][N+:2]([CH3:20])([CH3:1])[CH2:4][CH:5]1[C:17](=[O:18])[C:16]2[C:15]3[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=3)[NH:9][C:8]=2[CH2:7][CH2:6]1

Participants

3

Reactant 2

HCID 6328Methyl iodideHCID 20185207HCID 20185207, compound

Product 1

HCID 20185208HCID 20185208, compound

Procedure

A solution of 3-[(dimethylamino)methyl]-1,2,3,9-tetrahydro-4H-carbazol-4-one (0.53 g) in iodomethane (15 ml) was heated under reflux for 5 h and evaporated to dryness, giving the title compound as a white solid (0.84 g) m.p. 202°-205°.

Workup

  1. temperatureunder reflux for 5 h
  2. customevaporated to dryness

Sources & evidence

ORD record
ord-172f083fbf2a40408ac6fa37cc126864
Source dataset
uspto-grants-1987_09
Patent number
US04695578

Reaction notes

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