HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13935155, compound → 1-Acridinol, 1,2,3,4-tetrahydro-9-amino-6-(trifluoromethyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13935155 | HCID 13935155 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 1-Acridinol, 1,2,3,4-tetrahydro-9-amino-6-(trifluoromethyl)- | HCID 3025608 | — |
Reaction Steps
9-Amino-3,4-dihydro-6-trifluoromethylacridin-1(2H)-one (2.4 g) was suspended in 60 ml of tetrahydrofuran. To this cooled solution was added 9 ml of 1 molar solution of lithium aluminum hydride in THF. This was stirred for 30 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04695573 |
| Source dataset | uspto-grants-1987_09 |
| ORD ID | ord-329b4c6c8bde480791b913b9ffc83c3c |
| Source note | uspto-grants-1987_09 |