HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13935147, compound → 104628-42-4
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13935147 | HCID 13935147 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 104628-42-4 | HCID 3025628 | — |
Reaction Steps
To a cooled solution of 4.2 g of 3,4-dihydro-9-[4,4-bis(4-fluorophenyl)butylamino]acridin-1(2H)-one in tetrahyddrofuran was added 5 ml of 1M solution of lithium aluminum hydride in tetrahydrofuran. This was stirred for 0.5 hour at ice bath temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04695573 |
| Source dataset | uspto-grants-1987_09 |
| ORD ID | ord-9953027407844da9903dee744fb839a0 |
| Source note | uspto-grants-1987_09 |