HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phthaloyl chloride → Bis[4-(propoxycarbonyl)phenyl] benzene-1,2-dicarboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phthaloyl chloride | HCID 6955 | — |
| Reactant | Propylparaben | HCID 7175 | — |
| Product | Bis[4-(propoxycarbonyl)phenyl] benzene-1,2-dicarboxylate | HCID 13878974 | — |
Reaction Steps
Propyl p-hydroxybenzoate and phthalic dichloride are allowed to react and treated in a similar procedure to Example 4. The residue obtained is recrystallized from hexane and recrystallized from ethyl acetate-chloroform (1:1) to yield di(p-propoxycarbonylphenyl)phthalate, m.p. 87°-89° C., as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04695649 |
| Source dataset | uspto-grants-1987_09 |
| ORD ID | ord-429982acbd98459c8a6290f2311aaa7b |
| Source note | uspto-grants-1987_09 |