2,2'-Bi-1H-benzimidazole → HCID 21245441, compound

HRID 2309675Notes

Reaction equation

HRID 2309675 reaction equation
[CH2:1]([O:14][C:15](Cl)=[O:16])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13].[CH:18]1[CH:23]=[C:22]2[NH:24][C:25]([C:27]3[NH:35][C:34]4[C:29](=[CH:30][CH:31]=[CH:32][CH:33]=4)[N:28]=3)=[N:26][C:21]2=[CH:20][CH:19]=1>>[CH2:1]([O:14][C:15]([N:35]1[C:34]2[CH:33]=[CH:32][CH:31]=[CH:30][C:29]=2[N:28]=[C:27]1[C:25]1[N:24]([C:15]([O:14][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13])=[O:16])[C:22]2[CH:23]=[CH:18][CH:19]=[CH:20][C:21]=2[N:26]=1)=[O:16])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13]

Participants

3

Reactant 2

HCID 2490972,2'-Bi-1H-benzimidazoleHCID 22026198HCID 22026198, compound

Product 1

HCID 21245441HCID 21245441, compound

Procedure

Following the procedure of Example 2, tridecylchloroformate was reacted with 2,2'-bibenzimidazole to give 1,1'-bis(tridecyloxycarbonyl)-2,2'- bibenzimidazole in 86% purity.

Sources & evidence

ORD record
ord-e6178611e8ea4ede949b9976d6967c3a
Source dataset
uspto-grants-1987_09
Patent number
US04696801

Reaction notes

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