HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propyl Isothiocyanate → HCID 53930108, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propyl Isothiocyanate | HCID 69403 | — |
| Reactant | HCID 13883776 | HCID 13883776 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 53930108 | HCID 53930108 | — |
Reaction Steps
A solution of 5-(3-aminopyrazol-1-yl)valeronitrile (1.0 g.) in acetonitrile (10 ml.) was treated with n-propylisothiocyanate (0.74 g.) and the solution heated under reflux on the steam bath for 6 hours. Evaporation of the solvent gave a brown gum which on trituration with ether/EtOH gave 5-(3-[3-propylthioureido]pyrazol-1-yl)valeronitrile as a white solid (1.01 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04696933 |
| Source dataset | uspto-grants-1987_09 |
| ORD ID | ord-c6ad5f8ce05d423186a9a62f7e743d6f |
| Source note | uspto-grants-1987_09 |