1-(4-Methoxyphenyl)-2-phenylethan-1-one → HCID 20067716, compound

HRID 2309763Notes

Reaction equation

[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]([CH2:11][C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)=[O:10])=[CH:5][CH:4]=1.[O:18]1[CH2:23][CH2:22][CH2:21][CH2:20][CH:19]1[O:24][CH:25]1[CH2:30]CCCO1.BrC(O)C>>[O:18]1[CH2:23][CH2:22][CH2:21][CH2:20][CH:19]1[O:24][CH2:25][CH2:30][CH:11]([C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)[C:9]([C:6]1[CH:5]=[CH:4][C:3]([O:2][CH3:1])=[CH:8][CH:7]=1)=[O:10]

Participants

Reactant 3

HCID 2310931-(4-Methoxyphenyl)-2-phenylethan-1-one

HCID 263182Tetrahydropyranyl ether

HCID 14202443Ethanol, 1-bromo-

Product 1

HCID 20067716HCID 20067716, compound

Procedure

The compound is prepared from 22.6 g of 4-methoxydesoxybenzoin and 20.9 g of tetrahydropyran-2-yl ether-protected bromoethanol according to the procedure described in Example 1(a).

Sources & evidence

ORD record: ord-47511eb935a843ceadca7e850b8a0ea4
Source dataset: uspto-grants-1987_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04696949

Reaction notes

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