HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isobutanol → HCID 15481774, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isobutanol | HCID 6560 | — |
| Reactant | N-Phenylacetyl-L-leucine | HCID 11983894 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 15481774 | HCID 15481774 | — |
Reaction Steps
N-Phenylacetyl-L-leucine (0.0081 g, 0.038 mmol) was dissolved in 2.0 mL CHCl3 (EtOH free) and iso-butyl alcohol (0.055 mL) and treated with P-EPC (100 mg, 0.87 milliequivalents). The mixture was rotated for 4 days, filtered through a plug of cotton and the filtrate evaporated at reduced pressure to an oil which was sufficiently pure for testing.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06849650B2 |
| Source dataset | uspto-grants-2005_02 |
| ORD ID | ord-3e99e35af0dc4e44b84f850154f8b329 |
| Source note | uspto-grants-2005_02 |