Sodium Acetate → HCID 53937978, compound

HRID 230988Notes

Reaction equation

HRID 230988 reaction equation
[C:1]([CH:6]1[C:11](=[O:12])[CH2:10][CH:9]([C:13]2[CH:18]=[CH:17][C:16]([CH2:19][CH2:20][CH3:21])=[CH:15][CH:14]=2)[CH2:8][C:7]1=[O:22])(=O)[CH2:2][CH2:3][CH3:4].[Cl-].[CH2:24]([O:26][NH3+:27])[CH3:25].C([O-])(=O)C.[Na+]>C(O)C>[CH2:24]([O:26][NH:27][CH2:4][CH2:3][CH2:2][CH:1]=[C:6]1[C:7](=[O:22])[CH2:8][CH:9]([C:13]2[CH:14]=[CH:15][C:16]([CH2:19][CH2:20][CH3:21])=[CH:17][CH:18]=2)[CH2:10][C:11]1=[O:12])[CH3:25]

Participants

5

Reactant 3

HCID 517045Sodium AcetateHCID 19001768HCID 19001768, compoundHCID 20034301HCID 20034301, compound

Product 1

HCID 53937978HCID 53937978, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

15.0 parts by weight of 2-butyryl-5-(4-n-propylphenyl)-cyclohexane-1,3-dione is reacted with 5.1 parts by weight of ethoxyammonium chloride and 4.5 parts by weight of anhydroud sodium acetate in 120 parts by volume of ethanol, and worked up as in Example 1. There is obtained 2-(ethoxyaminobutylidene)-5-(4-n-propylphenyl)-cyclohexane-1,3-dione (active ingredient No. 4).

Sources & evidence

ORD record
ord-358edaca31a04663ad2729d3df526781
Source dataset
uspto-grants-1989_07
Patent number
US04844735

Reaction notes

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