Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethylamine → 8-(2'-Methoxy-4'-dimethylaminosulfonyl-phenyl)-purine hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethylamine | HCID 674 | — |
| 반응물 | 4,5-Diaminopyrimidine | HCID 83703 | — |
| 반응물 | 4-(Chlorosulfonyl)-2-methoxybenzoic acid | HCID 20184580 | — |
| 생성물 | 8-(2'-Methoxy-4'-dimethylaminosulfonyl-phenyl)-purine hydrochloride | HCID 20184581 | — |
반응 단계
Prepared analogously to Example 51 from 2-methoxy-4-chlorosulfonyl-benzoic acid, aqueous dimethylamine solution, and 4,5-diamino-pyrimidine. The hydrochloride was recrystallized from ethanol/water (4:1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04696931 |
| 출처 데이터셋 | uspto-grants-1987_09 |
| ORD ID | ord-3bb5f706d3d94f2c9efb7c7c2bb57798 |
| 출처 메모 | uspto-grants-1987_09 |