HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 4'-(16-Hydroxyhexadecyloxy)biphenyl-4-carboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 4'-(16-Acetyloxyhexadecyloxy)biphenyl-4-carboxylic acid ethyl ester | HCID 54184442 | — |
| Solvent | Water | HCID 962 | — |
| Product | 4'-(16-Hydroxyhexadecyloxy)biphenyl-4-carboxylic acid | HCID 19859977 | 95.6% |
Reaction Steps
30 m moles(15.7 g) of the above 4'-(16-acetyloxyhexadecyloxy)biphenyl-4-carboxylic acid ethyl ester and 10 g of sodium hydroxide were stirred for 10 min. at 70° C. in a mixed solution of 40 ml of ethanol and 80 ml of water. After the reaction, the reaction solution was concentrated to obtain 13.0 g of 4'-(16-hydroxyhexadecyloxy)biphenyl-4-carboxylic acid. (yield: 95%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04844835 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-c2bcd08f64654292b3d26c7e768364f5 |
| Source note | uspto-grants-1989_07 |