HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Cyanocinnamyl alcohol → 3-(3-Hydroxypropyl)benzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Cyanocinnamyl alcohol | HCID 53735247 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-(3-Hydroxypropyl)benzonitrile | HCID 13854262 | — |
Reaction Steps
A solution of 3-cyanocinnamyl alcohol (4.1 g) in methanol (100 ml) was hydrogenated at 50 psi over 10% palladium on charcoal (0.5 g) for 1 hour. The catalyst was filtered off and the filtrate was evaporated to give the product as a pale oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04845110 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-e79787e0295e49e08590d53b358ed62a |
| Source note | uspto-grants-1989_07 |