HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(3-Cyanophenyl)-2-propenoic acid → 3-Cyanobenzenepropanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(3-Cyanophenyl)-2-propenoic acid | HCID 44725869 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | 3-Cyanobenzenepropanoic acid | HCID 13854269 | — |
Reaction Steps
A solution of 3-cyano-cinnamic acid (11.5 g) in water (200 ml) and 2M sodium hydroxide solution (35 ml) was hydrogenated at 60 psi over 10% palladium on charcoal for 1.5 hours. The catalyst was filtered off and the filtrate was acidified with 2M hydrochloric acid to precipitate the product as a white solid, m.p. 103° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04845110 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-e0d85199d0754eb98fe2b02a4ba51a4d |
| Source note | uspto-grants-1989_07 |