HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → 3-[3-(Methoxycarbonyl)phenyl]propanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | HCID 53414976 | HCID 53414976 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Water | HCID 962 | — |
| Product | 3-[3-(Methoxycarbonyl)phenyl]propanoic acid | HCID 10035947 | — |
Reaction Steps
A solution of 3-methoxycarbonyl-cinnamic acid (15.0 g) and sodium carbonate (7.7 g) in water (200 ml) was hydrogenated at 50 psi over 10% palladium on charcoal (0.5 g) for 1.5 hours. The catalyst was filtered off and the filtrate was acidified with 2M hydrochloric acid to precipitate the product as a white solid, m.p. 81° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04845110 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-56405047724e46979b89c32ffed19c58 |
| Source note | uspto-grants-1989_07 |