HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20034698, compound → HCID 19887978, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20034698 | HCID 20034698 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19887978 | HCID 19887978 | — |
Reaction Steps
A mixture of 2.38 g of the compound of Example 1 as a 0.1M ethanol solution and 900 mg of 10% palladium on carbon was stirred, under a 50 psi. atmosphere of hydrogen gas, for 17 hours. The mixture was then filtered through Celite and the crude residue was flash chromatographed on silica gel employing ethyl acetate as the eluent to yield the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04845129 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-e32409c449714be3a754bf1e19bb2e60 |
| Source note | uspto-grants-1989_07 |