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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 231200Generated: October 31, 2026

HCID 20034698, compound → HCID 19887978, compound

https://huagongshe.com/reaction/231200

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 20034698HCID 20034698—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 19887978HCID 19887978—

Reaction Steps

A mixture of 2.38 g of the compound of Example 1 as a 0.1M ethanol solution and 900 mg of 10% palladium on carbon was stirred, under a 50 psi. atmosphere of hydrogen gas, for 17 hours. The mixture was then filtered through Celite and the crude residue was flash chromatographed on silica gel employing ethyl acetate as the eluent to yield the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04845129
Source datasetuspto-grants-1989_07
ORD IDord-e32409c449714be3a754bf1e19bb2e60
Source noteuspto-grants-1989_07